S-ethyl bis(ethylsulfanyl)(4-isobutylphenyl)thioacetate

Base Information

Chemical Name:S-ethyl bis(ethylsulfanyl)(4-isobutylphenyl)thioacetate
CAS No.:467225-71-4
Molecular Formula:C₁₈H₂₈OS₃
Molecular Weight:356.618
Hs Code.:

Synonyms:S-ethyl bis(ethylsulfanyl)(4-isobutylphenyl)thioacetate

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Chemical Property of S-ethyl bis(ethylsulfanyl)(4-isobutylphenyl)thioacetate

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Technology Process of S-ethyl bis(ethylsulfanyl)(4-isobutylphenyl)thioacetate

There total 2 articles about S-ethyl bis(ethylsulfanyl)(4-isobutylphenyl)thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 467225-66-7
2,2,2-tris(ethylsulfanyl)-1-(4-isobutylphenyl)ethanone

: 467225-71-4
S-ethyl bis(ethylsulfanyl)(4-isobutylphenyl)thioacetate

Guidance literature:: With triphenylmethyl perchlorate; In dichloromethane; at 20 - 25 ℃; for 2h;
DOI:10.1055/s-2002-28521

Reference yield:

: 154320-56-6
methyl 4-iso-butylbenzoate

: 467225-71-4
S-ethyl bis(ethylsulfanyl)(4-isobutylphenyl)thioacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi / tetrahydrofuran; hexane / 2 h / -95 °C

1.2: 94 percent / tetrahydrofuran; hexane / 0.08 h / -95 °C

2.1: 89 percent / trityl perchlorate / CH₂Cl₂ / 2 h / 20 - 25 °C

With n-butyllithium; triphenylmethyl perchlorate; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1055/s-2002-28521

Reference yield: 81.0%

: 77-78-1
dimethyl sulfate

: 467225-71-4
S-ethyl bis(ethylsulfanyl)(4-isobutylphenyl)thioacetate

: 467225-75-8
S-ethyl α-(4-isobutylphenyl)-α-(ethylsulfanyl)thiopropionate

Guidance literature:: S-ethyl bis(ethylsulfanyl)(4-isobutylphenyl)thioacetate; With potassium tert-butylate; In tetrahydrofuran; at 20 - 25 ℃; for 0.166667h;

dimethyl sulfate; In tetrahydrofuran; at 20 - 25 ℃; for 0.5h;
DOI:10.1055/s-2002-28521