N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide

Base Information

• Chemical Name: N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide
• CAS No.: 954374-12-0
• Molecular Formula: C₅₆H₄₃N₃O₁₀
• Molecular Weight: 917.972
• Mol file: 954374-12-0.mol

Synonyms:N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide

Chemical Property of N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide

There total 1 articles about N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

5-nitro-1,3-benzenedicarbonylchloride (13438-30-7) + 2-amino-1-(4-tert-butylphenoxy)anthracene-9,10-dione (68256-56-4) → N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide (954374-12-0)

Guidance literature:

In toluene; for 0.5h; Heating;

DOI:10.1134/S1070428006110145

Reference yield: 92.0%

N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide (954374-12-0) + p-toluidine (106-49-0,12221-03-3) → N,N'-bis[1-hydroxy-9-(4-methylphenyl)imine-9,10-anthraquinon-2-yl]-5-nitroisophthalamide

Guidance literature:

In benzene; at 20 - 25 ℃; UV-irradiation;

DOI:10.1134/S1070428006110145

Reference yield: 60.0%

N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide (954374-12-0) → 5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide (954374-13-1)

Guidance literature:

With hydrazine hydrate; palladium on activated charcoal; In ethanol; for 1h; Heating;

DOI:10.1134/S1070428006110145

upstream raw materials:

5-nitro-1,3-benzenedicarbonylchloride

2-amino-1-(4-tert-butylphenoxy)anthracene-9,10-dione

Downstream raw materials:

5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide