5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide

Base Information

• Chemical Name: 5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide
• CAS No.: 954374-13-1
• Molecular Formula: C₅₆H₄₅N₃O₈
• Molecular Weight: 887.989

Synonyms:5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide

Chemical Property of 5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide

Chemical Property:

Purity/Quality:

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Technology Process of 5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide

There total 3 articles about 5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide (954374-12-0) → 5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide (954374-13-1)

Guidance literature:

With hydrazine hydrate; palladium on activated charcoal; In ethanol; for 1h; Heating;

DOI:10.1134/S1070428006110145

Reference yield:

5-nitro-1,3-benzenedicarbonylchloride (13438-30-7) → 5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide (954374-13-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / toluene / 0.5 h / Heating

2: 60 percent / hydrazine hydrate / Pd/C / ethanol / 1 h / Heating

With hydrazine hydrate; palladium on activated charcoal; In ethanol; toluene;

DOI:10.1134/S1070428006110145

Reference yield:

2-amino-1-(4-tert-butylphenoxy)anthracene-9,10-dione (68256-56-4) → 5-amino-N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]isophthalamide (954374-13-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / toluene / 0.5 h / Heating

2: 60 percent / hydrazine hydrate / Pd/C / ethanol / 1 h / Heating

With hydrazine hydrate; palladium on activated charcoal; In ethanol; toluene;

DOI:10.1134/S1070428006110145

upstream raw materials:

N,N'-bis[1-(4-tert-butylphenoxy)-9,10-anthraquinon-2-yl]-5-nitroisophthalamide

5-nitro-1,3-benzenedicarbonylchloride

2-amino-1-(4-tert-butylphenoxy)anthracene-9,10-dione

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