Technology Process of 3-
propanal
There total 15 articles about 3-propanal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-(5-((3R,5S)-5-(diphenyl(trimethylsilyloxy)methyl)pyrrolidin-3-yloxy)-5-oxopentyl)-1-methyl-1H-imidazol-3-ium hexafluorophosphate;
In
aq. ethanol;
at 4 ℃;
for 48h;
optical yield given as %ee;
enantioselective reaction;
DOI:10.1002/ejoc.200900807
- Guidance literature:
-
diethyl malonate;
With
lithium hydroxide monohydrate;
In
dichloromethane;
at 20 ℃;
for 0.0833333h;
C16H16O3;
With
(2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine;
In
dichloromethane;
at 20 ℃;
for 2h;
Solvent;
Temperature;
enantioselective reaction;
Catalytic behavior;
DOI:10.1055/s-0035-1561397
- Guidance literature:
-
3-Phenylpropenol;
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; copper(l) chloride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 1h;
under 760.051 Torr;
diethyl malonate;
With
(2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; benzoic acid;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 18h;
Reagent/catalyst;
stereoselective reaction;
