tert-butyl 4-acetoxybenzoate

Base Information

• Chemical Name: tert-butyl 4-acetoxybenzoate
• CAS No.: 59854-09-0
• Molecular Formula: C₁₃H₁₆O₄
• Molecular Weight: 236.268

Synonyms:tert-butyl 4-acetoxybenzoate

Chemical Property of tert-butyl 4-acetoxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of tert-butyl 4-acetoxybenzoate

There total 2 articles about tert-butyl 4-acetoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

tert-butyl 4-hydroxybenzoate (25804-49-3) + acetyl chloride (75-36-5) → tert-butyl 4-acetoxybenzoate (59854-09-0)

Guidance literature:

With pyridine; In tetrahydrofuran; at 0 - 20 ℃; for 16.25h; Inert atmosphere;

DOI:10.1021/acs.joc.6b02931

Reference yield:

4-acetoxybenzoyl chloride (27914-73-4) + tert-butyl alcohol (75-65-0) → tert-butyl 4-acetoxybenzoate (59854-09-0)

Guidance literature:

With pyridine; In ethyl acetate;

Reference yield:

tert-butyl 4-acetoxybenzoate (59854-09-0) → 4-acetoxybenzoyl chloride (27914-73-4)

Guidance literature:

With thionyl chloride; water; at 23 ℃; for 16h; Sealed tube;

DOI:10.1021/acs.joc.6b02931

upstream raw materials:

4-acetoxybenzoyl chloride

tert-butyl alcohol

tert-butyl 4-hydroxybenzoate

acetyl chloride

Downstream raw materials:

tert-butyl 4-hydroxybenzoate

4-acetoxybenzoyl chloride

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