2’-(trifluoromethyl)-3’,4’,5’-trimethoxyacetophenone

Base Information

Chemical Name:2’-(trifluoromethyl)-3’,4’,5’-trimethoxyacetophenone
CAS No.:1446436-57-2
Molecular Formula:C₁₂H₁₃F₃O₄
Molecular Weight:278.228
Hs Code.:

Synonyms:2’-(trifluoromethyl)-3’,4’,5’-trimethoxyacetophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2’-(trifluoromethyl)-3’,4’,5’-trimethoxyacetophenone

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Technology Process of 2’-(trifluoromethyl)-3’,4’,5’-trimethoxyacetophenone

There total 4 articles about 2’-(trifluoromethyl)-3’,4’,5’-trimethoxyacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1136-86-3
methyl (3,4,5-trimethoxyphenyl) ketone

: 2926-29-6
Langlois reagent

: 1446436-57-2
2’-(trifluoromethyl)-3’,4’,5’-trimethoxyacetophenone

Guidance literature:: With acetic anhydride; acetone; at 20 ℃; for 20h; Reagent/catalyst; UV-irradiation; Inert atmosphere;
DOI:10.1021/jacs.6b02782

Reference yield: 61.0%

: 1136-86-3
methyl (3,4,5-trimethoxyphenyl) ketone

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 1446436-57-2
2’-(trifluoromethyl)-3’,4’,5’-trimethoxyacetophenone

Guidance literature:: With [bis(acetoxy)iodo]benzene; silver fluoride; In dimethyl sulfoxide; at 20 ℃; for 20h;
DOI:10.1039/c3cc41829d

Reference yield: 47.0%

: 1136-86-3
methyl (3,4,5-trimethoxyphenyl) ketone

: 75-63-8
Bromotrifluoromethane

: 1446436-57-2
2’-(trifluoromethyl)-3’,4’,5’-trimethoxyacetophenone

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium diacetate; caesium carbonate; catacxium A; In acetone; at 130 ℃; for 40h; regioselective reaction; Inert atmosphere; Autoclave;
DOI:10.1002/anie.201511131