1-(2-methylphenyloxyacetyl)-4-(4-chlorophenyloxyacetyl)-thiosemicarbazide

Base Information

Chemical Name:1-(2-methylphenyloxyacetyl)-4-(4-chlorophenyloxyacetyl)-thiosemicarbazide
CAS No.:325139-77-3
Molecular Formula:C₁₈H₁₈ClN₃O₄S
Molecular Weight:407.878
Hs Code.:

Synonyms:1-(2-methylphenyloxyacetyl)-4-(4-chlorophenyloxyacetyl)-thiosemicarbazide

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Chemical Property of 1-(2-methylphenyloxyacetyl)-4-(4-chlorophenyloxyacetyl)-thiosemicarbazide

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Technology Process of 1-(2-methylphenyloxyacetyl)-4-(4-chlorophenyloxyacetyl)-thiosemicarbazide

There total 2 articles about 1-(2-methylphenyloxyacetyl)-4-(4-chlorophenyloxyacetyl)-thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 36304-37-7
o-tolyloxyacetic acid hydrazide

: 58903-20-1
4-chlorophenyloxyacetyl isothiocyanate

: 325139-77-3
1-(2-methylphenyloxyacetyl)-4-(4-chlorophenyloxyacetyl)-thiosemicarbazide

Guidance literature:: In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1080/00397910008087084

Reference yield:

: 4122-68-3
4-chlorophenyloxyacetyl chloride

: 325139-77-3
1-(2-methylphenyloxyacetyl)-4-(4-chlorophenyloxyacetyl)-thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: PEG-400 / CH₂Cl₂ / 1 h / 20 °C

2: 86 percent / CH₂Cl₂ / 0.5 h / 20 °C

With PEG-400; In dichloromethane;
DOI:10.1080/00397910008087084