4-(1-(Methoxycarbonyl)cyclopropyl)phenylboronic acid

Base Information

• Chemical Name: 4-(1-(Methoxycarbonyl)cyclopropyl)phenylboronic acid
• CAS No.: 1217501-08-0
• Molecular Formula: C₁₁H₁₃BO₄
• Molecular Weight: 220.033
• Hs Code.: 2931900090
• Mol file: 1217501-08-0.mol

Synonyms:(4-(1-(methoxycarbonyl)cyclopropyl)phenyl)boronic acid

Chemical Property of 4-(1-(Methoxycarbonyl)cyclopropyl)phenylboronic acid

Chemical Property:

• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-(1-(Methoxycarbonyl)cyclopropyl)phenylboronicacid ^*data from reagent suppliers

Safty Information:

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Technology Process of 4-(1-(Methoxycarbonyl)cyclopropyl)phenylboronic acid

There total 1 articles about 4-(1-(Methoxycarbonyl)cyclopropyl)phenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

diphenyl(vinyl)sulfonium trifluoromethanesulfonate + [4-(2-methoxy-2-oxoethyl)phenyl]boronic acid (454185-96-7) → (4-(1-(methoxycarbonyl)cyclopropyl)phenyl)boronic acid (1217501-08-0)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dimethyl sulfoxide; at 21 ℃; for 12h;

DOI:10.1016/j.tetlet.2018.02.080

Reference yield: 71.0%

(4-(1-(methoxycarbonyl)cyclopropyl)phenyl)boronic acid (1217501-08-0) + 2‐ethenyl‐N‐(quinolin‐8‐yl)benzamide (1578268-89-9) → methyl 1-(4-(2-fluoro-2-(2-(quinolin-8-ylcarbamoyl)phenyl)ethyl)phenyl)cyclopropanecarboxylate (1578268-53-7)

Guidance literature:

With Bis(2-ethylhexyl)phosphoric acid; 4-tert-Butylcatechol; palladium diacetate; Selectfluor; 4,4'-di-tert-butyl-2,2'-bipyridine; In dichloromethane; water; at 20 ℃; Inert atmosphere;

DOI:10.1021/ja412881j

Reference yield: 53.0%

4-(4-bromophenyl)-4H-[1,2,4]triazol-3-ylamine (1396007-86-5) + (4-(1-(methoxycarbonyl)cyclopropyl)phenyl)boronic acid (1217501-08-0) → 1-[4'-(3-amino-[1,2,4]triazol-4-yl)-biphenyl-4-yl]-cyclopropanecarboxylic acid methyl ester (1396007-98-9)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In 1,4-dioxane; water; at 100 ℃; for 24h; Inert atmosphere;

upstream raw materials:

[4-(2-methoxy-2-oxoethyl)phenyl]boronic acid

Downstream raw materials:

1-[4'-(3-amino-[1,2,4]triazol-4-yl)-biphenyl-4-yl]-cyclopropanecarboxylic acid methyl ester

4-(4'-(1-(methoxycarbonyl)cyclopropyl)-[1,1'-biphenyl]-4-yl)-1-methyl-1H-imidazole-5-carbaldehyde

1-{3'-fluoro-4'-[1-methyl-5-((R)-1-phenylethoxycarbonylamino)-1H-[1,2,3]triazole-4-yl]biphenyl-4-yl}cyclopropanecarboxylic acid

methyl 1-(4-(2-fluoro-2-(2-(quinolin-8-ylcarbamoyl)phenyl)ethyl)phenyl)cyclopropanecarboxylate

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