Technology Process of 1,3,5-tris-(1,2,2,3-tetramethyl-cyclopentanecarbonyl)-benzene
There total 10 articles about 1,3,5-tris-(1,2,2,3-tetramethyl-cyclopentanecarbonyl)-benzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 77 percent / tetrahydrofuran / 5 h / Ambient temperature
2: 28 percent / Dibromobis(tri-n-butylphosphan)nickel(II) / hexane / 36 h / Heating
3: Jones reagent / acetone / 2 h / Ambient temperature
With
jones reagent;
dibromobis(tri-n-butylphosphan)nickel(II);
In
tetrahydrofuran; hexane; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 83 percent / LiAlH4 / diethyl ether / 4 h / Heating
2: 91 percent / pyridinium chlorochromate / CH2Cl2 / 1.5 h / Ambient temperature
3: 77 percent / tetrahydrofuran / 5 h / Ambient temperature
4: 28 percent / Dibromobis(tri-n-butylphosphan)nickel(II) / hexane / 36 h / Heating
5: Jones reagent / acetone / 2 h / Ambient temperature
With
lithium aluminium tetrahydride; jones reagent; pyridinium chlorochromate;
dibromobis(tri-n-butylphosphan)nickel(II);
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; acetone;