2-phenyl>-4,4-dimethyloxazoline

Base Information

Chemical Name:2-phenyl>-4,4-dimethyloxazoline
CAS No.:84694-19-9
Molecular Formula:C₂₁H₃₃NOSi
Molecular Weight:343.585
Hs Code.:

2-<o-<1-(trimethylsilyl)hept-6-enyl>phenyl>-4,4-dimethyloxazoline

Synonyms:2-phenyl>-4,4-dimethyloxazoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenyl>-4,4-dimethyloxazoline

Chemical Property:

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Technology Process of 2-phenyl>-4,4-dimethyloxazoline

There total 1 articles about 2-phenyl>-4,4-dimethyloxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 18922-04-8
6-iodohex-1-ene

: 84694-18-8
2-{o-[(trimethylsilyl)methyl]phenyl}-4,4-dimethyloxazoline

: 84694-19-9
2-phenyl>-4,4-dimethyloxazoline

Guidance literature:: With n-butyllithium; 1.) ether, hexane, 0 deg C, 30 min, 2.) HMPA, RT, overnight;
DOI:10.1021/ja00344a028

Reference yield: 90.0%

: 84694-19-9
2-phenyl>-4,4-dimethyloxazoline

: 74-88-4
methyl iodide

: 84694-24-6
2-phenyl>-3,4,4-trimethyloxazolinium iodide

Guidance literature:: In acetonitrile; at 40 - 50 ℃; for 7h;
DOI:10.1021/ja00344a028

Reference yield:

: 84694-19-9
2-phenyl>-4,4-dimethyloxazoline

: 84694-27-9
2-phenyl>-3-methyl-4(S)-methyl-5(R)-phenyloxazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / acetonitrile / 7 h / 40 - 50 °C

2: 1.) NaBH₄, Et₃N, 2.) 5percent HCl / 1.) EtOH, -78 deg C, 1 min, 2.) -78 deg C -> RT, 3 h

With hydrogenchloride; sodium tetrahydroborate; triethylamine; In acetonitrile;
DOI:10.1021/ja00344a028