5-(4-cyclopropyl-1H-imidazol-1-yl)-2-methoxybenzoic acid hydrochloride

Base Information

Chemical Name:5-(4-cyclopropyl-1H-imidazol-1-yl)-2-methoxybenzoic acid hydrochloride
CAS No.:1354412-93-3
Molecular Formula:C₁₄H₁₄N₂O₃*ClH
Molecular Weight:294.738
Hs Code.:

Synonyms:5-(4-cyclopropyl-1H-imidazol-1-yl)-2-methoxybenzoic acid hydrochloride

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Chemical Property of 5-(4-cyclopropyl-1H-imidazol-1-yl)-2-methoxybenzoic acid hydrochloride

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Technology Process of 5-(4-cyclopropyl-1H-imidazol-1-yl)-2-methoxybenzoic acid hydrochloride

There total 4 articles about 5-(4-cyclopropyl-1H-imidazol-1-yl)-2-methoxybenzoic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1354412-91-1
isopropyl 5-(4-cyclopropyl-1H-imidazol-1-yl)-2-methoxy-benzoate

: 1354412-93-3
5-(4-cyclopropyl-1H-imidazol-1-yl)-2-methoxybenzoic acid hydrochloride

Guidance literature:: With hydrogenchloride; water; at 100 ℃; for 10h;

Reference yield:

: 2786-00-7
2-methoxy-5-iodobenzoic acid

: 1354412-93-3
5-(4-cyclopropyl-1H-imidazol-1-yl)-2-methoxybenzoic acid hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / Inert atmosphere

2: dichloromethane / 0.25 h

3: caesium carbonate; 8-quinolinol / copper(I) oxide / butyronitile / 16 h / 120 °C / Inert atmosphere

4: hydrogenchloride; water / 10 h / 100 °C

With hydrogenchloride; 8-quinolinol; oxalyl dichloride; water; caesium carbonate; N,N-dimethyl-formamide; copper(I) oxide; In dichloromethane; butyronitile;

Reference yield:

: 115860-69-0
2-methoxy-5-iodobenzoyl chloride

: 1354412-93-3
5-(4-cyclopropyl-1H-imidazol-1-yl)-2-methoxybenzoic acid hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 0.25 h

2: caesium carbonate; 8-quinolinol / copper(I) oxide / butyronitile / 16 h / 120 °C / Inert atmosphere

3: hydrogenchloride; water / 10 h / 100 °C

With hydrogenchloride; 8-quinolinol; water; caesium carbonate; copper(I) oxide; In dichloromethane; butyronitile;