N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide

Base Information

• Chemical Name: N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide
• CAS No.: 1065638-48-3
• Molecular Formula: C₁₉H₂₅ClN₂OS₂
• Molecular Weight: 397.005

Synonyms:N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide

Chemical Property of N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide

Chemical Property:

Purity/Quality:

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Technology Process of N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide

There total 1 articles about N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzamide (1065639-63-5) → N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide (1065638-48-3)

Guidance literature:

With Lawessons reagent; In toluene; at 80 ℃; for 0.5h;

Reference yield:

CYANAMID (420-04-2) + N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide (1065638-48-3) → N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-N'-cyano-2-methoxybenzenecarboximidamide (1065638-49-4)

Guidance literature:

With triethylamine; mercury(II) diacetate; In acetonitrile; at 80 ℃; for 0.75h;

Reference yield:

N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide (1065638-48-3) + ethylhydrazine carboxylate (4114-31-2) → ethyl Z-2-[{[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]amino}(5-chloro-2-methoxyphenyl)methylene]hydrazinecarboxylate (1065638-92-7) + ethyl E-2-[{[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]amino}(5-chloro-2-methoxyphenyl)methylene]hydrazinecarboxylate (1065638-94-9)

Guidance literature:

With acetic acid; mercury(II) diacetate; In 1,4-dioxane; at 80 ℃; for 2h;

upstream raw materials:

N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzamide

Downstream raw materials:

N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-N'-cyano-2-methoxybenzenecarboximidamide

ethyl Z-2-[{[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]amino}(5-chloro-2-methoxyphenyl)methylene]hydrazinecarboxylate

ethyl E-2-[{[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]amino}(5-chloro-2-methoxyphenyl)methylene]hydrazinecarboxylate

N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-hydroxybenzenecarbothioamide

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