N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-hydroxybenzenecarbothioamide

Base Information

• Chemical Name: N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-hydroxybenzenecarbothioamide
• CAS No.: 1065640-16-5
• Molecular Formula: C₁₈H₂₃ClN₂OS₂
• Molecular Weight: 382.978

Synonyms:N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-hydroxybenzenecarbothioamide

Chemical Property of N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-hydroxybenzenecarbothioamide

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Technology Process of N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-hydroxybenzenecarbothioamide

There total 1 articles about N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-hydroxybenzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide (1065638-48-3) → N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-hydroxybenzenecarbothioamide (1065640-16-5)

Guidance literature:

With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield:

N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-hydroxybenzenecarbothioamide (1065640-16-5) + carbamic acid phenyl ester (622-46-8) → 2-{{[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]amino}[(phenoxycarbonyl)imino]methyl}-4-chlorophenyl acetate (1065638-85-8)

Guidance literature:

With triethylamine; mercury(II) diacetate; In acetonitrile; at 80 ℃; for 0.75h;

Reference yield:

bromo-acetic acid amide (683-57-8) + N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-hydroxybenzenecarbothioamide (1065640-16-5) → 2-(2-{[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]carbamothioyl}-4-chlorophenoxy)acetamide (1231955-31-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 72h;

upstream raw materials:

N-[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]-5-chloro-2-methoxybenzenecarbothioamide

Downstream raw materials:

2-{{[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]amino}[(phenoxycarbonyl)imino]methyl}-4-chlorophenyl acetate

2-(2-{[(2Z)-3-butyl-5-tert-butyl-1,3-thiazol-2(3H)-ylidene]carbamothioyl}-4-chlorophenoxy)acetamide

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