Rh(5,10,15,20-tetramesitylporphyrinato)SiMe₃

Base Information

Chemical Name:Rh(5,10,15,20-tetramesitylporphyrinato)SiMe₃
CAS No.:823834-99-7
Molecular Formula:C₅₉H₆₁N₄RhSi
Molecular Weight:957.151
Hs Code.:

Rh(5,10,15,20-tetramesitylporphyrinato)SiMe<sub>3</sub>

Synonyms:Rh(5,10,15,20-tetramesitylporphyrinato)SiMe₃

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Chemical Property of Rh(5,10,15,20-tetramesitylporphyrinato)SiMe₃

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Technology Process of Rh(5,10,15,20-tetramesitylporphyrinato)SiMe₃

There total 3 articles about Rh(5,10,15,20-tetramesitylporphyrinato)SiMe₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 110-86-1
pyridine

: 121393-39-3
5,10,15,20-tetra(2,4,6-trimethylphenyl)porphyrinate rhodium(II)

: 7677-24-9
trimethylsilyl cyanide

: 823835-01-4
(pyridine)Rh(5,10,15,20-tetramesitylporphyrinato)CN

: 823834-99-7
Rh(5,10,15,20-tetramesitylporphyrinato)SiMe₃

Guidance literature:: In benzene; High Pressure; N2, 2 equiv. pyridine, 10 equiv. silyl cyanide, 110°C, 1 h;
DOI:10.1021/om049253h

Reference yield: 79.0%

: 121393-39-3
5,10,15,20-tetra(2,4,6-trimethylphenyl)porphyrinate rhodium(II)

: 7677-24-9
trimethylsilyl cyanide

: [Rh(meso-tetramesitylporphyrinato)(CN)]

: 823834-99-7
Rh(5,10,15,20-tetramesitylporphyrinato)SiMe₃

Guidance literature:: With triphenylphosphine; In not given; a soln. of P(C6H5)3 added to a soln. of Rh complex at room temp., Si compd. added, heated at 110°C for 3 h under N2 in the absence of light; chromd. (silica gel, hexane/CH2Cl2);
DOI:10.1021/om0605276

Reference yield:

: 110-86-1
pyridine

: (5,10,15,20-tetra(2,4,6-trimethylphenyl)porphyrinate)rhodium(III) methyl

: 7677-24-9
trimethylsilyl cyanide

: 823835-01-4
(pyridine)Rh(5,10,15,20-tetramesitylporphyrinato)CN

: 823834-99-7
Rh(5,10,15,20-tetramesitylporphyrinato)SiMe₃

Guidance literature:: In benzene; Irradiation (UV/VIS); a soln. of Rh complex photolyzed, reacted with Si compd. and C5H5N in C6H6 at 60-90°C; not isolated, detected by UV-vis; Kinetics;
DOI:10.1021/om0605276