1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol

Base Information

Chemical Name:1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol
CAS No.:1191953-73-7
Molecular Formula:C₃₃H₄₄O₅Si
Molecular Weight:548.795
Hs Code.:

Synonyms:1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol

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Chemical Property of 1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol

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Technology Process of 1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol

There total 1 articles about 1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 942155-68-2
2D-(2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethylsilyl)tetrahydroxycyclohexanone

: 1191953-73-7
1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.bmc.2009.07.025

Reference yield: 100.0%

: 1191953-73-7
1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol

: 74-88-4
methyl iodide

: 1191953-76-0
1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethylsilyl)-1-O-methylcyclohexanepentol

Guidance literature:: 1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.166667h;

methyl iodide; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2009.07.025

Reference yield:

: 1191953-73-7
1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol

: 100-39-0
benzyl bromide

: 1191953-74-8
1D-(1,2,3/4,5)-1,2,3,4-tetra-O-benzyl-5-O-(tert-butyldimethylsilyl)cyclohexanepentol

Guidance literature:: 1D-(1,2,3/4,5)-2,3,4-tri-O-benzyl-5-O-(tert-butyldimethsilyl)cyclohexanepentol; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2009.07.025