2-ethoxy-1-phenylbut-3-enyl isobutyrate

Base Information

Chemical Name:2-ethoxy-1-phenylbut-3-enyl isobutyrate
CAS No.:934668-02-7
Molecular Formula:C₁₆H₂₂O₃
Molecular Weight:262.349
Hs Code.:

Synonyms:2-ethoxy-1-phenylbut-3-enyl isobutyrate

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Chemical Property of 2-ethoxy-1-phenylbut-3-enyl isobutyrate

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Technology Process of 2-ethoxy-1-phenylbut-3-enyl isobutyrate

There total 3 articles about 2-ethoxy-1-phenylbut-3-enyl isobutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 257861-23-7
3-Ethoxy-4-hydroxy-4-phenyl-1-buten

: 79-30-1
isobutyryl chloride

: 934668-02-7
2-ethoxy-1-phenylbut-3-enyl isobutyrate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/ol062933r

Reference yield:

: 557-31-3
3-ethoxyprop-1-ene

: 934668-02-7
2-ethoxy-1-phenylbut-3-enyl isobutyrate

Guidance literature:: Multi-step reaction with 2 steps

1.1: s-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: InCl₃ / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.3: 90 percent / tetrahydrofuran; hexane / -78 - 20 °C

2.1: 86 percent / Et₃N / CH₂Cl₂ / 20 °C

With sec.-butyllithium; triethylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol062933r

Reference yield:

: 100-52-7
benzaldehyde

: 934668-02-7
2-ethoxy-1-phenylbut-3-enyl isobutyrate

Guidance literature:: Multi-step reaction with 2 steps

1.1: s-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: InCl₃ / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.3: 90 percent / tetrahydrofuran; hexane / -78 - 20 °C

2.1: 86 percent / Et₃N / CH₂Cl₂ / 20 °C

With sec.-butyllithium; triethylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol062933r