2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide)

Base Information

Chemical Name:2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide)
CAS No.:1286252-33-2
Molecular Formula:C₃₄H₃₆N₂O₆
Molecular Weight:568.67
Hs Code.:

Synonyms:2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide)

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Chemical Property of 2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide)

Chemical Property:

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Technology Process of 2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide)

There total 1 articles about 2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 20919-36-2
N-benzylsalicylamide

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 1286252-33-2
2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide)

Guidance literature:: N-benzylsalicylamide; With potassium carbonate; In N,N-dimethyl-formamide; for 1h; Heating;

triethylene glycol di-(p-toluenesulfonate); In N,N-dimethyl-formamide; for 24h; Reflux;
DOI:10.1039/c1dt10931f

Reference yield:

: 1286252-33-2
2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide)

: 141-78-6
ethyl acetate

: erbium(III) nitrate

: Er₂(NO₃)6(2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide))3*2(ethyl acetate)

Guidance literature:: In methanol; ethyl acetate; soln. of metal salt in MeOH added to soln. of ligand in ethyl acetate, stirred for 4 h at room temp.; filtered, washed with ethyl acetate, dried in vac. over P2O5 for 24 h, ppt. dissolved in MeOH/ethyl acetate, filtered, crystd. at room temp. for2 wk;
DOI:10.1039/c1dt10931f

Reference yield:

: 1286252-33-2
2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide)

: 141-78-6
ethyl acetate

: 16454-60-7
neodymium(III) nitrate

: Nd₂(NO₃)6(2,2'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)bis(N-benzylbenzamide))3*2(ethyl acetate)

Guidance literature:: In methanol; ethyl acetate; soln. of metal salt in MeOH added to soln. of ligand in ethyl acetate, stirred for 4 h at room temp.; filtered, washed with ethyl acetate, dried in vac. over P2O5 for 24 h, ppt. dissolved in MeOH/ethyl acetate, filtered, crystd. at room temp. for2 wk;
DOI:10.1039/c1dt10931f