N-(5-oxo-2-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-4-yl)-L-phenylalaninamide

Base Information

Chemical Name:N-(5-oxo-2-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-4-yl)-L-phenylalaninamide
CAS No.:1345014-71-2
Molecular Formula:C₂₃H₂₂N₄O₂
Molecular Weight:386.453
Hs Code.:

Synonyms:N-(5-oxo-2-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-4-yl)-L-phenylalaninamide

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Chemical Property of N-(5-oxo-2-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-4-yl)-L-phenylalaninamide

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Technology Process of N-(5-oxo-2-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-4-yl)-L-phenylalaninamide

There total 3 articles about N-(5-oxo-2-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-4-yl)-L-phenylalaninamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 5241-58-7
L-Phenylalanine amide

: 1345014-05-2
tert-butyl 4-(methylsulfonyl)-5-oxo-2-phenyl-7,8-dihydro-1,6-naphthyridine-6(5H)-carboxylate

: 1345014-71-2
N-(5-oxo-2-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-4-yl)-L-phenylalaninamide

Guidance literature:: at 70 - 160 ℃; microwave irradiation;

Reference yield:

: 1345013-92-4
tert-butyl 3-[bis(methylthio)methylene]-2,4-dioxopiperidine-1-carboxylate

: 1345014-71-2
N-(5-oxo-2-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-4-yl)-L-phenylalaninamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / dimethyl sulfoxide; tetrahydrofuran / 2.5 h

1.2: 2 h / 90 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2.5 h / 5 - 20 °C

3.1: 70 - 160 °C / microwave irradiation

With potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1345013-95-7
tert-butyl 4-(methylthio)-5-oxo-2-phenyl-7,8-dihydro-1,6-naphthyridine-6(5H)-carboxylate

: 1345014-71-2
N-(5-oxo-2-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-4-yl)-L-phenylalaninamide

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2.5 h / 5 - 20 °C

2: 70 - 160 °C / microwave irradiation

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;