1-methyl-4-piperazinecarboxamidine hydrogen sulfate

Base Information

Chemical Name:1-methyl-4-piperazinecarboxamidine hydrogen sulfate
CAS No.:84727-42-4
Molecular Formula:C₆H₁₄N₄*H₂O₄S
Molecular Weight:240.283
Hs Code.:

Synonyms:1-methyl-4-piperazinecarboxamidine hydrogen sulfate

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Chemical Property of 1-methyl-4-piperazinecarboxamidine hydrogen sulfate

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Technology Process of 1-methyl-4-piperazinecarboxamidine hydrogen sulfate

There total 1 articles about 1-methyl-4-piperazinecarboxamidine hydrogen sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-01-3
1-methyl-piperazine

: 867-44-7,147895-43-0
S-Methylisothiourea sulfate

: 28457-20-7,84727-42-4
N-methylpiperazine carboxamidine sulfate

Guidance literature:: In water; for 0.25h; Heating;
DOI:10.1016/j.bmcl.2005.04.011 DOI:10.1016/j.bmcl.2005.04.014

Reference yield: 93.0%

: 21739-93-5
2-bromo-5-chlorobenzoic acid

: 28457-20-7,84727-42-4
N-methylpiperazine carboxamidine sulfate

: 33017-92-4
6-chloro-2-(4-methylpiperazin-1-yl)quinazolin-4(3H)-one

Guidance literature:: 2-bromo-5-chlorobenzoic acid; N-methylpiperazine carboxamidine sulfate; With caesium carbonate; In N,N-dimethyl-formamide; for 0.333333h; Inert atmosphere;

With copper(l) iodide; caesium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 40h; Inert atmosphere;
DOI:10.1055/s-0029-1216871

Reference yield: 86.0%

: 115351-30-9
3-anilino-2-(4-chlorophenyl)-3-methylthioacrylonitrile

: 84727-42-4
1-methyl-4-piperazinecarboxamidine hydrogen sulfate

: 1178005-81-6
C₂₁H₂₃ClN₆

Guidance literature:: 1-methyl-4-piperazinecarboxamidine hydrogen sulfate; With sodium; In ethanol; at 70 ℃; for 3h;

3-anilino-2-(4-chlorophenyl)-3-methylthioacrylonitrile; In ethanol; N,N-dimethyl-formamide; for 7h; Reflux;