dexamethasone 21-(p-nitrophenyl carbonate)

Base Information

Chemical Name:dexamethasone 21-(p-nitrophenyl carbonate)
CAS No.:79360-11-5
Molecular Formula:C₂₉H₃₂FNO₉
Molecular Weight:557.573
Hs Code.:

Synonyms:dexamethasone 21-(p-nitrophenyl carbonate)

Suppliers and Price of dexamethasone 21-(p-nitrophenyl carbonate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dexamethasone 21-(p-nitrophenyl carbonate)

Chemical Property:

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Technology Process of dexamethasone 21-(p-nitrophenyl carbonate)

There total 1 articles about dexamethasone 21-(p-nitrophenyl carbonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 50-02-2
dexamethasone

: 7693-46-1
4-Nitrophenyl chloroformate

: 79360-11-5
dexamethasone 21-(p-nitrophenyl carbonate)

Guidance literature:: With pyridine; In chloroform; Ambient temperature;
DOI:10.1021/jm00144a004

Reference yield: 76.0%

: tranexamic acid

: 79360-11-5
dexamethasone 21-(p-nitrophenyl carbonate)

: C₃₁H₄₂FNO₈

Guidance literature:: With 4-methyl-morpholine; In dimethyl sulfoxide; at 30 ℃; for 20h;

Reference yield:

: 79360-11-5
dexamethasone 21-(p-nitrophenyl carbonate)

: (6-Amino-hexyl)-carbamic acid 2-((8S,9R,10S,11S,13S,14S,16R,17R)-9-fluoro-11,17-dihydroxy-10,13,16-trimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-17-yl)-2-oxo-ethyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / N-methylmorpholine / dimethylformamide / 24 h / 20 °C

2: 71 percent / acetonitrile / 24 h / 20 °C

With 4-methyl-morpholine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(01)01291-6