2-Chloro-4-iodo-3-methylpyridine

Base Information

Chemical Name:2-Chloro-4-iodo-3-methylpyridine
CAS No.:153034-88-9
Molecular Formula:C6H5ClIN
Molecular Weight:253.47
Hs Code.:2933399090
European Community (EC) Number:675-069-9
DSSTox Substance ID:DTXSID90435387
Nikkaji Number:J566.228A
Wikidata:Q72452487
Mol file:153034-88-9.mol

Synonyms:2-Chloro-4-iodo-3-methylpyridine;153034-88-9;2-Chloro-4-iodo-3-picoline;2-chloro-4-iodo-3-methyl-pyridine;2-chloro-3-methyl-4-iodopyridine;Pyridine, 2-chloro-4-iodo-3-methyl-;MFCD03095293;SCHEMBL1117775;DTXSID90435387;WHCRABJNJRAJIP-UHFFFAOYSA-N;AKOS015851090;AB13660;AM62374;CS-W009353;2-Chloro-4-iodo-3-methylpyridine, 97%;AC-33395;DS-13257;SY022301;C3368;FT-0691618;EN300-106188;A809377

Suppliers and Price of 2-Chloro-4-iodo-3-methylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-chloro-4-iodo-3-methylpyridine
10mg
$ 45.00

TCI Chemical
2-Chloro-4-iodo-3-methylpyridine >98.0%(GC)
1g
$ 111.00

TCI Chemical
2-Chloro-4-iodo-3-methylpyridine >98.0%(GC)
5g
$ 378.00

SynQuest Laboratories
2-Chloro-4-iodo-3-methylpyridine 97%
5 g
$ 167.00

SynQuest Laboratories
2-Chloro-4-iodo-3-methylpyridine 97%
1 g
$ 45.00

Sigma-Aldrich
2-Chloro-4-iodo-3-methylpyridine 97%
500mg
$ 74.00

Matrix Scientific
2-Chloro-4-iodo-3-methylpyridine
250mg
$ 396.00

Labseeker
2-Chloro-4-iodo-3-methylpyridine 95
25g
$ 585.00

J&W Pharmlab
2-Chloro-4-iodo-3-methyl-pyridine 96%
25g
$ 398.00

J&W Pharmlab
2-Chloro-4-iodo-3-methyl-pyridine 96%
5g
$ 120.00

Total 53 raw suppliers

Chemical Property of 2-Chloro-4-iodo-3-methylpyridine

Chemical Property:

Vapor Pressure:0.009mmHg at 25°C
Melting Point:101-106 °C
Refractive Index:1.624
Boiling Point:274.895 °C at 760 mmHg
PKA:0.58±0.10(Predicted)
Flash Point:120.053 °C
PSA：12.89000
Density:1.906 g/cm³
LogP:2.64800
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C
Sensitive.:Light Sensitive
Solubility.:soluble in Toluene
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:252.91552
Heavy Atom Count:9
Complexity:99.1

Purity/Quality:

99% ^*data from raw suppliers

2-chloro-4-iodo-3-methylpyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 22-41
Safety Statements: 26-39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CN=C1Cl)I

Technology Process of 2-Chloro-4-iodo-3-methylpyridine

There total 1 articles about 2-Chloro-4-iodo-3-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 78607-36-0
2-chloro-3-iodopyridine

: 74-88-4
methyl iodide

: 153034-88-9
2-chloro-4-iodo-3-methyl-pyridine

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; 1.) -75 deg C, 3 h, 2.) -75 deg C, 2 h;
DOI:10.1021/jo00079a031

Reference yield: 92.0%

: 153034-88-9
2-chloro-4-iodo-3-methyl-pyridine

: 98-80-6
phenylboronic acid

: 2-chloro-3-methyl-4-phenylpyridine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In water; tert-butyl alcohol; at 80 ℃; for 2h; Inert atmosphere;