N-[2-N'-(9-fluorenylmethyloxycarbonyl)aminobenzenesulfonyl]-N-methyl-L-serine methyl ester

Base Information

Chemical Name:N-[2-N'-(9-fluorenylmethyloxycarbonyl)aminobenzenesulfonyl]-N-methyl-L-serine methyl ester
CAS No.:369617-58-3
Molecular Formula:C₂₆H₂₆N₂O₇S
Molecular Weight:510.568
Hs Code.:

Synonyms:N-[2-N'-(9-fluorenylmethyloxycarbonyl)aminobenzenesulfonyl]-N-methyl-L-serine methyl ester

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Chemical Property of N-[2-N'-(9-fluorenylmethyloxycarbonyl)aminobenzenesulfonyl]-N-methyl-L-serine methyl ester

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Technology Process of N-[2-N'-(9-fluorenylmethyloxycarbonyl)aminobenzenesulfonyl]-N-methyl-L-serine methyl ester

There total 1 articles about N-[2-N'-(9-fluorenylmethyloxycarbonyl)aminobenzenesulfonyl]-N-methyl-L-serine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 369617-57-2
N-(2-aminobenzenesulfonyl)-N-methyl-L-serine methyl ester

: 369617-58-3
N-[2-N'-(9-fluorenylmethyloxycarbonyl)aminobenzenesulfonyl]-N-methyl-L-serine methyl ester

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/S0040-4020(01)00658-5

Reference yield: 73.0%

: 369617-58-3
N-[2-N'-(9-fluorenylmethyloxycarbonyl)aminobenzenesulfonyl]-N-methyl-L-serine methyl ester

: 369617-59-4
methyl 2-N-[[2-N'-(9-fluorenylmethyloxycarbonyl)aminobenzenesulfonyl]methylamino]acrylate

Guidance literature:: With trifluoromethylsulfonic anhydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/S0040-4020(01)00658-5

Reference yield:

: 369617-58-3
N-[2-N'-(9-fluorenylmethyloxycarbonyl)aminobenzenesulfonyl]-N-methyl-L-serine methyl ester

: 369617-60-7
methyl 2-N-[(2-aminobenzenesulfonyl)methylamino]acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / DIEA; Tf₂O / CH₂Cl₂ / 2 h / 20 °C

2: 70 percent / DIEA / CH₂Cl₂ / 48 h / Heating

With trifluoromethylsulfonic anhydride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4020(01)00658-5