Technology Process of C70H86N2O8
There total 4 articles about C70H86N2O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sulfuric acid
2: potassium carbonate / acetone
3: sodium hydroxide / ethanol; water / 0.08 h / Microwave irradiation
4: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C / Reflux
5: tetrahydrofuran / 3 h / 20 °C
With
oxalyl dichloride; sulfuric acid; potassium carbonate; N,N-dimethyl-formamide; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetone;
DOI:10.1080/10610278.2013.817578
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / ethanol; water / 0.08 h / Microwave irradiation
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C / Reflux
3: tetrahydrofuran / 3 h / 20 °C
With
oxalyl dichloride; N,N-dimethyl-formamide; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1080/10610278.2013.817578