N₁-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl)-1,2-benzenediamine

Base Information

Chemical Name:N₁-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl)-1,2-benzenediamine
CAS No.:219492-87-2
Molecular Formula:C₁₈H₂₃N₅O
Molecular Weight:325.414
Hs Code.:

N<sub>1</sub>-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl)-1,2-benzenediamine

Synonyms:N₁-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl)-1,2-benzenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₁-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl)-1,2-benzenediamine

Chemical Property:

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Technology Process of N₁-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl)-1,2-benzenediamine

There total 5 articles about N₁-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl)-1,2-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 219492-86-1
2-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl]amino-nitrobenzene

: 219492-87-2
N₁-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl)-1,2-benzenediamine

Guidance literature:: With hydrogen; 10percent Pd/C; In ethanol;
DOI:10.1021/jm990625b

Reference yield:

: 3320-86-3
2-nitrophenyl isocyanate

: 219492-87-2
N₁-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl)-1,2-benzenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃; tetrahydrofuran

2: H₂ / 10percent Pd/C / ethanol

With hydrogen; 10percent Pd/C; In tetrahydrofuran; ethanol; chloroform; 1: Condensation / 2: Reduction;
DOI:10.1021/jm990625b

Reference yield:

: 121912-29-6
1-(pyridin-4-yl)piperidine-4-carboxylic acid ethyl ester

: 219492-87-2
N₁-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl)-1,2-benzenediamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: LiAlH₄

2.1: phthalimide; diethylazodicarboxylate; Ph₃P / tetrahydrofuran

2.2: hydrazine monohydrate / ethanol / 70 °C

3.1: CHCl₃; tetrahydrofuran

4.1: H₂ / 10percent Pd/C / ethanol

With lithium aluminium tetrahydride; phthalimide; hydrogen; triphenylphosphine; diethylazodicarboxylate; 10percent Pd/C; In tetrahydrofuran; ethanol; chloroform; 1.1: Reduction / 2.1: Mitsunobu reaction / 2.2: Decomposition / 3.1: Condensation / 4.1: Reduction;
DOI:10.1021/jm990625b