(2S,3R)-(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl 3-((methoxycarbonyl)amino)-2,3-diphenylpropanoate

Base Information

Chemical Name:(2S,3R)-(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl 3-((methoxycarbonyl)amino)-2,3-diphenylpropanoate
CAS No.:1609238-06-3
Molecular Formula:C₃₃H₃₉NO₄
Molecular Weight:513.677
Hs Code.:

Synonyms:(2S,3R)-(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl 3-((methoxycarbonyl)amino)-2,3-diphenylpropanoate

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Chemical Property of (2S,3R)-(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl 3-((methoxycarbonyl)amino)-2,3-diphenylpropanoate

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Technology Process of (2S,3R)-(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl 3-((methoxycarbonyl)amino)-2,3-diphenylpropanoate

There total 1 articles about (2S,3R)-(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl 3-((methoxycarbonyl)amino)-2,3-diphenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 960-71-4
triphenylborane

: 27593-61-9
methyl N-phenylmethylenecarbamate

: 180036-72-0
(1R,2S,5R)-phenylmenthyl diazoacetate

: 1609238-06-3
(2S,3R)-(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl 3-((methoxycarbonyl)amino)-2,3-diphenylpropanoate

Guidance literature:: In dichloromethane; at -10 ℃; for 24h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo5003505

Reference yield: 76.0%

: 1609238-06-3
(2S,3R)-(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl 3-((methoxycarbonyl)amino)-2,3-diphenylpropanoate

: C₁₆H₁₉NO

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/jo5003505

Reference yield:

: 1609238-06-3
(2S,3R)-(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl 3-((methoxycarbonyl)amino)-2,3-diphenylpropanoate

: (4R,5S)-3-methyl-4,5-diphenyl-1,3-oxazinan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0.08 h / 0 - 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 10 h / -78 - 20 °C / Inert atmosphere

With dmap; lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo5003505