3-<(3S,4R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutyryl>-2-thiazolidinethione

Base Information

Chemical Name:3-<(3S,4R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutyryl>-2-thiazolidinethione
CAS No.:138694-10-7
Molecular Formula:C₁₇H₂₂N₂O₆S₂
Molecular Weight:414.503
Hs Code.:

Synonyms:3-<(3S,4R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutyryl>-2-thiazolidinethione

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Chemical Property of 3-<(3S,4R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutyryl>-2-thiazolidinethione

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Technology Process of 3-<(3S,4R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutyryl>-2-thiazolidinethione

There total 6 articles about 3-<(3S,4R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutyryl>-2-thiazolidinethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 96-53-7
2-mercaptothiazoline

: 138694-15-2
(4R,3R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutaoic acid

: 138694-10-7
3-<(3S,4R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutyryl>-2-thiazolidinethione

Guidance literature:: With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 25 ℃;
DOI:10.1021/jo00030a006

Reference yield: 84.0%

: 134469-06-0
thiazolidine-2-thione

: 138694-15-2
(4R,3R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutaoic acid

: 138694-10-7
3-<(3S,4R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutyryl>-2-thiazolidinethione

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 24h;
DOI:10.1021/jo00054a035

Reference yield:

: 138694-13-0
(2R,3R)-(2,5-Dimethoxy-3-nitrophenyl)-3-methoxy-2-methylpropionic acid

: 138694-10-7
3-<(3S,4R)-4-(2,5-Dimethoxy-3-nitrophenyl)-4-methoxy-3-methylbutyryl>-2-thiazolidinethione

Guidance literature:: Multi-step reaction with 4 steps

1: (COCl)2, DMF / CH₂Cl₂ / 16 h / Ambient temperature

2: CH₂Cl₂; diethyl ether / 0.5 h / 0 °C

3: 87 percent / AgNO₃, H₂O / tetrahydrofuran / 23 h / 25 °C

4: 84 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide*HCl, DMAP / CH₂Cl₂ / 24 h

With dmap; oxalyl dichloride; water; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo00054a035