3,5-bis-[(tert-butyldimethylsilyl)oxy]-4-[(trimethylsilyl)oxy]cyclohexanol benzyl ether

Base Information

Chemical Name:3,5-bis-[(tert-butyldimethylsilyl)oxy]-4-[(trimethylsilyl)oxy]cyclohexanol benzyl ether
CAS No.:681830-91-1
Molecular Formula:C₂₈H₅₄O₄Si₃
Molecular Weight:538.991
Hs Code.:

Synonyms:3,5-bis-[(tert-butyldimethylsilyl)oxy]-4-[(trimethylsilyl)oxy]cyclohexanol benzyl ether

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Chemical Property of 3,5-bis-[(tert-butyldimethylsilyl)oxy]-4-[(trimethylsilyl)oxy]cyclohexanol benzyl ether

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Technology Process of 3,5-bis-[(tert-butyldimethylsilyl)oxy]-4-[(trimethylsilyl)oxy]cyclohexanol benzyl ether

There total 2 articles about 3,5-bis-[(tert-butyldimethylsilyl)oxy]-4-[(trimethylsilyl)oxy]cyclohexanol benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 100-39-0
benzyl bromide

: 681830-90-0
3,5-bis-[(tert-butyldimethylsilyl)oxy]-4-[(trimethylsilyl)oxy]cyclohexanol

: 681830-91-1
3,5-bis-[(tert-butyldimethylsilyl)oxy]-4-[(trimethylsilyl)oxy]cyclohexanol benzyl ether

Guidance literature:: DOI:10.1016/j.bmcl.2004.12.090

Reference yield:

: 141404-09-3
(3R,5R)-3,5-bis<(tert-butyldimethylsilyl)oxy>-4-<(trimethylsilyl)oxy>cyclohexanone

: 681830-91-1
3,5-bis-[(tert-butyldimethylsilyl)oxy]-4-[(trimethylsilyl)oxy]cyclohexanol benzyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / sodium borohydride / ethanol / 1.5 h / 0 °C

2: 85 percent / sodium hydride / dimethylformamide / 8 h / 0 °C

With sodium tetrahydroborate; sodium hydride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.01.061