(Z)-styrylsulfonyl acetic acid

Base Information Edit

Chemical Name:(Z)-styrylsulfonyl acetic acid
CAS No.:137325-91-8
Molecular Formula:C₁₀H₁₀O₄S
Molecular Weight:226.253
Hs Code.:
Mol file:137325-91-8.mol

Synonyms:(Z)-styrylsulfonyl acetic acid

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Chemical Property of (Z)-styrylsulfonyl acetic acid Edit

Chemical Property:

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Technology Process of (Z)-styrylsulfonyl acetic acid

There total 5 articles about (Z)-styrylsulfonyl acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 52147-97-4
trans 2-phenylethenesulfonyl chloride

: 79-11-8
chloroacetic acid

: 137325-91-8,102154-41-6
(Z)-styrylsulfonyl acetic acid

Guidance literature:: trans 2-phenylethenesulfonyl chloride; With sodium hydrogencarbonate; sodium sulfite; In water; at 80 - 90 ℃; for 1h;

chloroacetic acid; In water; for 3h; pH=10; Heating;

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 137325-91-8,102154-41-6
(Z)-styrylsulfonyl acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: 79 percent / SO₂Cl₂; N-methylpyrrolidine / 4 h / 90 °C

2.1: NaHCO₃; Na₂SO₃ / H₂O / 1 h / 80 - 90 °C

2.2: 63 percent / H₂O / 3 h / pH 10 / Heating

With 1-Methylpyrrolidine; sulfuryl dichloride; sodium hydrogencarbonate; sodium sulfite; In water; 1.1: Substitution / 2.1: Substitution / 2.2: Alkylation;