2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propan oic acid

Base Information

Chemical Name:2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propan oic acid
CAS No.:1225031-94-6
Molecular Formula:C₂₃H₁₆Br₂ClNO₆
Molecular Weight:597.644
Hs Code.:

Synonyms:2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propan oic acid

Suppliers and Price of 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propan oic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propan oic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propan oic acid

There total 7 articles about 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propan oic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1225032-38-1
Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate

: 1225031-94-6
2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propan oic acid

Guidance literature:: Ethyl 2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propanoate; With water; sodium hydroxide; In ethanol; at 50 ℃; for 2h;

With hydrogenchloride; In water; pH=4;

Reference yield:

: 150-76-5
4-methoxy-phenol

: 1225031-94-6
2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propan oic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 130 - 135 °C

2.1: hydroxylamine hydrochloride / ethanol; water / 2 h / 90 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 25 °C

4.1: Eaton′s Reagent / 16 h / 95 °C

5.1: boron tribromide / dichloromethane / -70 - -20 °C / Inert atmosphere

5.2: 0.17 h / 20 - 25 °C

6.1: sodium hydroxide; water / ethanol / 2 h / 50 °C

6.2: pH 4

With Eaton′s Reagent; hydroxylamine hydrochloride; water; boron tribromide; potassium carbonate; caesium carbonate; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1225032-66-5
ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate

: 1225031-94-6
2-(((3,5-dibromo-4-(3-(4-chlorobenzoyl)-4-hydroxy phenoxy)benzylidene)amino)oxy)propan oic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: Eaton′s Reagent / 16 h / 95 °C

2.1: boron tribromide / dichloromethane / -70 - -20 °C / Inert atmosphere

2.2: 0.17 h / 20 - 25 °C

3.1: sodium hydroxide; water / ethanol / 2 h / 50 °C

3.2: pH 4

With Eaton′s Reagent; water; boron tribromide; sodium hydroxide; In ethanol; dichloromethane;