ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate

Base Information

Chemical Name:ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate
CAS No.:1225032-66-5
Molecular Formula:C₁₉H₁₉Br₂NO₅
Molecular Weight:501.172
Hs Code.:

Synonyms:ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate

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Chemical Property of ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate

Chemical Property:

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Technology Process of ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate

There total 4 articles about ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1225032-65-4
3,5-dibromo-4-(4-methoxyphenoxy)benzaldehyde oxime

: 535-11-5,41978-69-2
Ethyl 2-bromopropionate

: 1225032-66-5
ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 2h;

Reference yield:

: 855264-88-9
3,5-dibromo-4-(4-methoxy-phenoxy)-benzaldehyde

: 1225032-66-5
ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride / ethanol; water / 2 h / 90 °C

2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 25 °C

With hydroxylamine hydrochloride; caesium carbonate; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 861787-50-0
3,5-dibromo-4-iodo-benzaldehyde

: 1225032-66-5
ethyl 2-(((3,5-dibromo-4-(4-methoxy phenoxy)benzylidene)amino)oxy)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 130 - 135 °C

2: hydroxylamine hydrochloride / ethanol; water / 2 h / 90 °C

3: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 25 °C

With hydroxylamine hydrochloride; potassium carbonate; caesium carbonate; In ethanol; water; N,N-dimethyl-formamide;