C₆₆H₁₁₁N₉O₂₁

Base Information

Chemical Name:C₆₆H₁₁₁N₉O₂₁
CAS No.:1566605-88-6
Molecular Formula:C₆₆H₁₁₁N₉O₂₁
Molecular Weight:1366.66
Hs Code.:

C<sub>66</sub>H<sub>111</sub>N<sub>9</sub>O<sub>21</sub>

Synonyms:C₆₆H₁₁₁N₉O₂₁

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₆H₁₁₁N₉O₂₁

Chemical Property:

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Technology Process of C₆₆H₁₁₁N₉O₂₁

There total 18 articles about C₆₆H₁₁₁N₉O₂₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 220156-99-0
benzyl (3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)carbamate

: 1566605-87-5
C₄₈H₈₃N₇O₁₇

: 1566605-88-6
C₆₆H₁₁₁N₉O₂₁

Guidance literature:: C₄₈H₈₃N₇O₁₇; With pyridine; acetic anhydride; at 20 ℃; for 2h; Inert atmosphere;

benzyl (3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)carbamate; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol500022n

Reference yield:

: 1566605-79-5
C₄₄H₆₇N₅O₁₄

: 1566605-88-6
C₆₆H₁₁₁N₉O₂₁

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 1 h / 20 °C / pH 8-9

2.1: palladium 10% on activated carbon; hydrogen / isopropyl alcohol / 2 h / 20 °C

3.1: acetic anhydride; pyridine / 2 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic anhydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; isopropyl alcohol;
DOI:10.1021/ol500022n

Reference yield:

: 1566605-91-1
1-methoxycarbonylmethyl-1-(4-nitrobenzenesulfonyl)-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane

: 1566605-88-6
C₆₆H₁₁₁N₉O₂₁

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate; thiophenol / acetonitrile / 4 h / 20 °C

2.1: potassium carbonate / acetonitrile / 72 h / 60 °C

3.1: hydrogenchloride / 1,4-dioxane / 5 h / 20 °C

4.1: acetic anhydride; pyridine / 2 h / 20 °C / Inert atmosphere

4.2: 15 h / 20 °C / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 1 h / 20 °C / pH 8-9

6.1: palladium 10% on activated carbon; hydrogen / isopropyl alcohol / 2 h / 20 °C

7.1: acetic anhydride; pyridine / 2 h / 20 °C / Inert atmosphere

7.2: 1 h / 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic anhydride; potassium carbonate; thiophenol; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; isopropyl alcohol; acetonitrile;
DOI:10.1021/ol500022n