5-methoxy-3-benzylpent-4-en-1-ol

Base Information

Chemical Name:5-methoxy-3-benzylpent-4-en-1-ol
CAS No.:462631-60-3
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:

Synonyms:5-methoxy-3-benzylpent-4-en-1-ol

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Chemical Property of 5-methoxy-3-benzylpent-4-en-1-ol

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Technology Process of 5-methoxy-3-benzylpent-4-en-1-ol

There total 1 articles about 5-methoxy-3-benzylpent-4-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20763-19-3
(methoxymethylene)triphenylphosphorane

: 68975-07-5,68975-13-3,68975-14-4,61129-28-0
3-benzyltetrahydrofuran-2-one

: 462631-60-3
5-methoxy-3-benzylpent-4-en-1-ol

Guidance literature:: 3-benzyltetrahydrofuran-2-one; With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at -40 - -5 ℃; for 1h;

(methoxymethylene)triphenylphosphorane; With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at 20 ℃; for 16h; Further stages.;
DOI:10.1021/ja026739l

Reference yield: 95.0%

: 67-56-1
methanol

: 462631-60-3
5-methoxy-3-benzylpent-4-en-1-ol

: 3-benzyl-2-(dimethoxymethyl)tetrahydrofuran

Guidance literature:: With 2,6-dimethylpyridine; tetraethylammonium tosylate; In tetrahydrofuran; Electrochemical reaction;
DOI:10.1021/ja001063k

Reference yield:

: 462631-60-3
5-methoxy-3-benzylpent-4-en-1-ol

: (2S,3S)-3-Benzyl-tetrahydro-furan-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: tertbutyllithium / tetrahydrofuran; pentane / -78 - 0 °C

1.2: tetrahydrofuran; pentane / 2 h / 20 °C

2.1: 0.970 g / tetrabutylammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

3.1: Et₄NOTs / Electrochemical reaction

3.2: 69 percent / Acid hydrolysis

With tetrabutyl ammonium fluoride; tert.-butyl lithium; tetraethylammonium tosylate; In tetrahydrofuran; pentane;
DOI:10.1021/ja026739l