1-phenoxyethyl dicyclohexylphosphinoselenothioate

Base Information

Chemical Name:1-phenoxyethyl dicyclohexylphosphinoselenothioate
CAS No.:1443532-65-7
Molecular Formula:C₂₀H₃₁OPSSe
Molecular Weight:429.465
Hs Code.:

Synonyms:1-phenoxyethyl dicyclohexylphosphinoselenothioate

Suppliers and Price of 1-phenoxyethyl dicyclohexylphosphinoselenothioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenoxyethyl dicyclohexylphosphinoselenothioate

Chemical Property:

Purity/Quality:

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Technology Process of 1-phenoxyethyl dicyclohexylphosphinoselenothioate

There total 3 articles about 1-phenoxyethyl dicyclohexylphosphinoselenothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 766-94-9
vinyl phenyl ether

: 14610-03-8
di(yclohexyl)phosphine sulfide

: 1443532-64-6
1-phenoxyethyl dicyclohexylphosphinothioselenoate

: 1443532-65-7
1-phenoxyethyl dicyclohexylphosphinoselenothioate

Guidance literature:: With selenium; In 1,4-dioxane; at 100 ℃; for 0.666667h; Overall yield = 93 %; Overall yield = 399 mg; Mechanism; Inert atmosphere;
DOI:10.1016/j.tet.2013.05.038

Reference yield:

: 766-94-9
vinyl phenyl ether

: 1427631-01-3
C₁₂H₂₃PSSe

: 1443532-64-6
1-phenoxyethyl dicyclohexylphosphinothioselenoate

: 1443532-65-7
1-phenoxyethyl dicyclohexylphosphinoselenothioate

Guidance literature:: With selenium; In 1,4-dioxane; at 20 - 25 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.tet.2013.05.038

Reference yield:

: 14610-03-8
di(yclohexyl)phosphine sulfide

: 1443532-64-6
1-phenoxyethyl dicyclohexylphosphinothioselenoate

: 1443532-65-7
1-phenoxyethyl dicyclohexylphosphinoselenothioate

Guidance literature:: Multi-step reaction with 2 steps

1: selenium / 1,4-dioxane / 100 °C / Inert atmosphere

2: selenium / 1,4-dioxane / 0.17 h / 20 - 25 °C / Inert atmosphere

With selenium; In 1,4-dioxane;
DOI:10.1016/j.tet.2013.05.038