α-Chlor-9-anisylidenfluoren

Base Information

• Chemical Name: α-Chlor-9-anisylidenfluoren
• CAS No.: 33686-68-9
• Molecular Formula: C₂₁H₁₅ClO
• Molecular Weight: 318.802
• Mol file: 33686-68-9.mol

Synonyms:α-Chlor-9-anisylidenfluoren

Chemical Property of α-Chlor-9-anisylidenfluoren

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-Chlor-9-anisylidenfluoren

There total 2 articles about α-Chlor-9-anisylidenfluoren which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-Anisylidene Dichlorid (33686-70-3) → α-Chlor-9-anisylidenfluoren (33686-68-9)

Guidance literature:

With acetic acid;

DOI:10.1021/jo00973a021

Reference yield:

p-methoxybenzylidene fluorene (2871-87-6) → α-Chlor-9-anisylidenfluoren (33686-68-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Cl₂

2: AcOH

With chlorine; acetic acid;

DOI:10.1021/jo00973a021

Reference yield:

methanol (67-56-1) + α-Chlor-9-anisylidenfluoren (33686-68-9) → 9-fluorenone (486-25-9,952573-42-1) + p-methoxybenzylidene fluorene (2871-87-6) + 9-[Methoxy-(4-methoxy-phenyl)-methylene]-9H-fluorene

Guidance literature:

Product distribution; Quantum yield; Ambient temperature; Irradiation; with/without O₂ addition; with/without AcCN solvent;

DOI:10.1021/j100089a027

upstream raw materials:

9-Anisylidene Dichlorid

p-methoxybenzylidene fluorene

Downstream raw materials:

9-fluorenone

p-methoxybenzylidene fluorene