2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropylacetamide

Base Information

• Chemical Name: 2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropylacetamide
• CAS No.: 1610614-20-4
• Molecular Formula: C₂₁H₁₆Cl₃F₃N₂OS₂
• Molecular Weight: 539.857

Synonyms:2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropylacetamide

Chemical Property of 2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropylacetamide

Chemical Property:

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Technology Process of 2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropylacetamide

There total 2 articles about 2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-cyclopropyl-2-mercaptoacetamide (886047-44-5) + 3-(3-chloro-4-fluoro-phenyl)-5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazole (1610614-72-6) → 2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropylacetamide (1610614-20-4)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6.5h;

Reference yield:

2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanylacetic acid (1610614-68-0) + Cyclopropylamine (765-30-0) → 2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropylacetamide (1610614-20-4)

Guidance literature:

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; at 80 ℃; for 16h;

Reference yield:

2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropylacetamide (1610614-20-4) → 2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropyl-acetamide (1610614-74-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h;

upstream raw materials:

2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanylacetic acid

Cyclopropylamine

N-cyclopropyl-2-mercaptoacetamide

3-(3-chloro-4-fluoro-phenyl)-5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazole

Downstream raw materials:

2-[2-chloro-4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]phenyl]sulfanyl-N-cyclopropyl-acetamide

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