Nα-[benzyloxycarbonyl]-N'-[5-tert-butoxycarbonyl-5-(bis[2-{bis(tert-butoxycarbonylmethyl)amino}ethyl]amino)pentyl]-L-phenylalaninamide

Base Information

Chemical Name:Nα-[benzyloxycarbonyl]-N'-[5-tert-butoxycarbonyl-5-(bis[2-{bis(tert-butoxycarbonylmethyl)amino}ethyl]amino)pentyl]-L-phenylalaninamide
CAS No.:1304777-57-8
Molecular Formula:C₅₅H₈₇N₅O₁₃
Molecular Weight:1026.32
Hs Code.:

Synonyms:Nα-[benzyloxycarbonyl]-N'-[5-tert-butoxycarbonyl-5-(bis[2-{bis(tert-butoxycarbonylmethyl)amino}ethyl]amino)pentyl]-L-phenylalaninamide

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Chemical Property of Nα-[benzyloxycarbonyl]-N'-[5-tert-butoxycarbonyl-5-(bis[2-{bis(tert-butoxycarbonylmethyl)amino}ethyl]amino)pentyl]-L-phenylalaninamide

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Technology Process of Nα-[benzyloxycarbonyl]-N'-[5-tert-butoxycarbonyl-5-(bis[2-{bis(tert-butoxycarbonylmethyl)amino}ethyl]amino)pentyl]-L-phenylalaninamide

There total 1 articles about Nα-[benzyloxycarbonyl]-N'-[5-tert-butoxycarbonyl-5-(bis[2-{bis(tert-butoxycarbonylmethyl)amino}ethyl]amino)pentyl]-L-phenylalaninamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1161-13-3
N-Cbz-L-Phe

: [N⁽²⁾,N⁽²⁾-bis[2-[bis(1,1-dimethylethoxy)-2-oxoethyl]amino]-ethyl]-L-lysine 1,1-dimethylethyl ester

: 1304777-57-8
Nα-[benzyloxycarbonyl]-N'-[5-tert-butoxycarbonyl-5-(bis[2-{bis(tert-butoxycarbonylmethyl)amino}ethyl]amino)pentyl]-L-phenylalaninamide

Guidance literature:: N-Cbz-L-Phe; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 0.333333h; Inert atmosphere;

[N⁽²⁾,N⁽²⁾-bis[2-[bis(1,1-dimethylethoxy)-2-oxoethyl]amino]-ethyl]-L-lysine 1,1-dimethylethyl ester; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201002976

Reference yield: 62.0%

: 1304777-57-8
Nα-[benzyloxycarbonyl]-N'-[5-tert-butoxycarbonyl-5-(bis[2-{bis(tert-butoxycarbonylmethyl)amino}ethyl]amino)pentyl]-L-phenylalaninamide

: 1304777-60-3
N'-[5-tert-butoxycarbonyl-5-(bis[2-{bis(tert-butoxycarbonylmethyl)amino}ethyl]amino)pentyl]-L-phenylalaninamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; acetic acid; In methanol; for 22h; under 3620.13 Torr;
DOI:10.1002/chem.201002976