C₃₂H₄₂O₃Si

Base Information

Chemical Name:C₃₂H₄₂O₃Si
CAS No.:1268269-12-0
Molecular Formula:C₃₂H₄₂O₃Si
Molecular Weight:502.769
Hs Code.:

C<sub>32</sub>H<sub>42</sub>O<sub>3</sub>Si

Synonyms:C₃₂H₄₂O₃Si

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Chemical Property of C₃₂H₄₂O₃Si

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Technology Process of C₃₂H₄₂O₃Si

There total 2 articles about C₃₂H₄₂O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1041002-59-8
(3S,4S)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-1-en-4-ol

: 2746-25-0
p-Methoxybenzyl bromide

: 1268269-12-0
C₃₂H₄₂O₃Si

Guidance literature:: (3S,4S)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-1-en-4-ol; With potassium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.333333h; Inert atmosphere;

p-Methoxybenzyl bromide; In tetrahydrofuran; mineral oil; for 12h; Inert atmosphere;
DOI:10.1021/ja200089f

Reference yield:

: 127793-62-8
4-((tert-butyldiphenylsilyl)oxy)butanal

: 1268269-12-0
C₃₂H₄₂O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; potassium tert-butylate / tetrahydrofuran / -78 - -45 °C / Inert atmosphere

1.2: -78 - -70 °C / Inert atmosphere

2.1: potassium hydride / tetrahydrofuran; mineral oil / 0.33 h / 20 °C / Inert atmosphere

2.2: 12 h / Inert atmosphere

With n-butyllithium; potassium tert-butylate; potassium hydride; In tetrahydrofuran; mineral oil; 1.1: Brown crotylboration / 1.2: Brown crotylboration;
DOI:10.1021/ja200089f

Reference yield:

: 1268269-12-0
C₃₂H₄₂O₃Si

: C₃₂H₄₄O₄Si

Guidance literature:: C₃₂H₄₂O₃Si; With dimethylsulfide borane complex; In tetrahydrofuran; at -10 - 20 ℃; for 7h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja200089f