1-(2,6-dichloro-phenyl)-2-[4-(N,N'-dimethyl-hydrazino)-2-methylsulfanyl-pyrimidin-5-yl]-ethanone

Base Information

Chemical Name:1-(2,6-dichloro-phenyl)-2-[4-(N,N'-dimethyl-hydrazino)-2-methylsulfanyl-pyrimidin-5-yl]-ethanone
CAS No.:909095-76-7
Molecular Formula:C₁₅H₁₆Cl₂N₄OS
Molecular Weight:371.29
Hs Code.:

1-(2,6-dichloro-phenyl)-2-[4-(<i>N</i>,<i>N</i>'-dimethyl-hydrazino)-2-methylsulfanyl-pyrimidin-5-yl]-ethanone

Synonyms:1-(2,6-dichloro-phenyl)-2-[4-(N,N'-dimethyl-hydrazino)-2-methylsulfanyl-pyrimidin-5-yl]-ethanone

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Chemical Property of 1-(2,6-dichloro-phenyl)-2-[4-(N,N'-dimethyl-hydrazino)-2-methylsulfanyl-pyrimidin-5-yl]-ethanone

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Technology Process of 1-(2,6-dichloro-phenyl)-2-[4-(N,N'-dimethyl-hydrazino)-2-methylsulfanyl-pyrimidin-5-yl]-ethanone

There total 6 articles about 1-(2,6-dichloro-phenyl)-2-[4-(N,N'-dimethyl-hydrazino)-2-methylsulfanyl-pyrimidin-5-yl]-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 909095-75-6
2-(4-chloro-2-methylsulfanylpyrimidin-5-yl)-1-(2,6-dichlorophenyl)ethanone

: 306-37-6
N,N'-Dimethylhydrazine dihydrochloride

: 909095-76-7
1-(2,6-dichloro-phenyl)-2-[4-(N,N'-dimethyl-hydrazino)-2-methylsulfanyl-pyrimidin-5-yl]-ethanone

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; Heating;
DOI:10.1016/j.bmcl.2006.05.072

Reference yield: 32.0%

: 909095-75-6
2-(4-chloro-2-methylsulfanylpyrimidin-5-yl)-1-(2,6-dichlorophenyl)ethanone

: 73664-86-5
1,2-dimethylhydrazine hydrochloride

: 909095-76-7
1-(2,6-dichloro-phenyl)-2-[4-(N,N'-dimethyl-hydrazino)-2-methylsulfanyl-pyrimidin-5-yl]-ethanone

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 100 ℃; for 2h;
DOI:10.3987/com-06-10806

Reference yield:

: 61044-96-0
4-chloro-5-methyl-2-(methylsulfanyl)pyrimidine

: 909095-76-7
1-(2,6-dichloro-phenyl)-2-[4-(N,N'-dimethyl-hydrazino)-2-methylsulfanyl-pyrimidin-5-yl]-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / N-bromosuccinimide / benzoyl peroxide / 1,2-dichloro-ethane / 2 h / Heating

2: 39 percent / LDA / tetrahydrofuran; heptane; ethylbenzene / 2 h / -78 °C

3: 32 percent / N,N-diisopropylethylamine / dimethylformamide / 2 h / 100 °C

With N-Bromosuccinimide; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; dibenzoyl peroxide; In tetrahydrofuran; n-heptane; ethylbenzene; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.3987/com-06-10806