2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one

Base Information

• Chemical Name: 2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one
• CAS No.: 1297309-88-6
• Molecular Formula: C₁₅H₁₅N₅OS
• Molecular Weight: 313.383

Synonyms:2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one

Chemical Property of 2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one

Chemical Property:

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Technology Process of 2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one

There total 2 articles about 2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide (1297309-74-0) + chloroacetic acid (79-11-8) → 2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one (1297309-88-6)

Guidance literature:

With sodium acetate; acetic acid; for 6h; Reflux;

DOI:10.1016/j.ejmech.2011.01.062

Reference yield:

methyl 5-methyl-2-phenyl-4-imidazolyl ketone (28824-91-1) → 2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one (1297309-88-6)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol; water / 5 h / Reflux

2: sodium acetate; acetic acid / 6 h / Reflux

With hydrogenchloride; sodium acetate; acetic acid; In ethanol; water;

DOI:10.1016/j.ejmech.2011.01.062

Reference yield: 48.0%

2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one (1297309-88-6) + 3-(1-benzofuran-2-yl)-1-phenyl-1H-pyrazole-4-carbaldehyde (372098-13-0) → 5-{[3-(benzofuran-2-yl)-1-phenyl-1H-pyrazol-4-yl]methylene}-2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one (1297309-94-4)

Guidance literature:

With sodium acetate; acetic acid; for 5h; Reflux;

DOI:10.1016/j.ejmech.2011.01.062

upstream raw materials:

2-(1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene)hydrazinecarbothioamide

chloroacetic acid

methyl 5-methyl-2-phenyl-4-imidazolyl ketone

Downstream raw materials:

5-(4-fluorobenzylidene)-2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one

2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}-5-((1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-4-yl)methylene)thiazolidin-4-one

5-{[3-(benzofuran-2-yl)-1-phenyl-1H-pyrazol-4-yl]methylene}-2-{[1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethylidene]hydrazono}thiazolidin-4-one

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