5-FLUORO-2-IODOBENZALDEHYDE

Base Information

Chemical Name:5-FLUORO-2-IODOBENZALDEHYDE
CAS No.:877264-44-3
Molecular Formula:C7H4FIO
Molecular Weight:250.011
Hs Code.:2913000090
Mol file:877264-44-3.mol

Synonyms:2-Iodo-5-fluorobenzaldehyde;

Suppliers and Price of 5-FLUORO-2-IODOBENZALDEHYDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
5-Fluoro-2-idoobenzaldehyde 97%
250 mg
$ 96.00

SynQuest Laboratories
5-Fluoro-2-idoobenzaldehyde 97%
1 g
$ 208.00

Matrix Scientific
5-Fluoro-2-iodobenzaldehyde 97%
1g
$ 488.00

Crysdot
5-Fluoro-2-iodobenzaldehyde 97%
5g
$ 1084.00

Atlantic Research Chemicals
5-Fluoro-2-iodobenzaldehyde 95%
1gm:
$ 187.33

American Custom Chemicals Corporation
2-IODO-5-FLUOROBENZALDEHYDE 95.00%
5G
$ 1673.60

Alichem
5-Fluoro-2-iodobenzaldehyde
5g
$ 1030.91

AK Scientific
5-Fluoro-2-iodobenzaldehyde
1g
$ 339.00

Total 36 raw suppliers

Chemical Property of 5-FLUORO-2-IODOBENZALDEHYDE

Chemical Property:

Vapor Pressure:0.0153mmHg at 25°C
Refractive Index:1.64
Boiling Point:256.6 °C at 760 mmHg
Flash Point:109 °C
PSA：17.07000
Density:1.962 g/cm³
LogP:2.24280
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

99%, ^*data from raw suppliers

5-Fluoro-2-idoobenzaldehyde 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-FLUORO-2-IODOBENZALDEHYDE

There total 5 articles about 5-FLUORO-2-IODOBENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 877264-43-2
(5-fluoro-2-iodophenyl)methanol

: 877264-44-3
5-fluoro-2-iodobenzaldehyde

Guidance literature:: With manganese(IV) oxide; In chloroform; for 18h; Reflux;

Reference yield:

: 319-24-4
2-amino-5-fluoro-benzoic acid methyl ester

: 877264-44-3
5-fluoro-2-iodobenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / acetonitrile / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / toluene / 2.5 h / -78 °C / Inert atmosphere

3.1: silica gel; pyridinium chlorochromate / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With silica gel; diisobutylaluminium hydride; toluene-4-sulfonic acid; pyridinium chlorochromate; In dichloromethane; toluene; acetonitrile;
DOI:10.1021/acs.orglett.8b02128

Reference yield:

: 52548-63-7
5-fluoro-2-iodobenzoic acid

: 877264-44-3
5-fluoro-2-iodobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 0 - 20 °C

2: pyridinium chlorochromate; silica gel / dichloromethane / 2 h / 0 - 20 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; silica gel; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3cc40577j