6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-5-hydroxy-5-methoxy-3-methyl-3H,5H-uracil

Base Information

Chemical Name:6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-5-hydroxy-5-methoxy-3-methyl-3H,5H-uracil
CAS No.:85894-82-2
Molecular Formula:C₁₇H₂₄N₄O₄
Molecular Weight:348.402
Hs Code.:

Synonyms:6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-5-hydroxy-5-methoxy-3-methyl-3H,5H-uracil

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Chemical Property of 6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-5-hydroxy-5-methoxy-3-methyl-3H,5H-uracil

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Technology Process of 6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-5-hydroxy-5-methoxy-3-methyl-3H,5H-uracil

There total 4 articles about 6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-5-hydroxy-5-methoxy-3-methyl-3H,5H-uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.8%

: 67-56-1
methanol

: 85894-81-1
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-5-hydroxy-3-methyluracil

: 85894-78-6
N,N',N',4,5-pentametyl-o-phenylenediamine

: 85894-82-2
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-5-hydroxy-5-methoxy-3-methyl-3H,5H-uracil

Guidance literature:: for 24h;
DOI:10.1021/ja00352a045

Reference yield:

: 18636-32-3
3-methyllumiflavin

: 85894-82-2
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-5-hydroxy-5-methoxy-3-methyl-3H,5H-uracil

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) dithionite, NaOH / 1.) aq. ethanol, ice bath, 1 h, 2.) room temperature; 50-55 deg C, 5 h

2: 30.2 percent / sodium hydrogen carbonate, m-chloroperbenzoic acid / CHCl₃ / 0.5 h

3: 70.5 percent / dithionite,aq. sodium chloride / CHCl₃ / 0.03 h / acetate buffer

4: 37.8 percent / 24 h

With sodium hydroxide; sodium dithionite; sodium hydrogencarbonate; dithionite^(2-); 3-chloro-benzenecarboperoxoic acid; sodium chloride; In chloroform;
DOI:10.1021/ja00352a045

Reference yield:

: 40815-89-2
3,5,5-trimethyl-1,5-dihydrolumiflavin

: 85894-82-2
6-<<2-(dimethylamino)-4,5-dimethylphenyl>methylamino>-5-hydroxy-5-methoxy-3-methyl-3H,5H-uracil

Guidance literature:: Multi-step reaction with 3 steps

1: 30.2 percent / sodium hydrogen carbonate, m-chloroperbenzoic acid / CHCl₃ / 0.5 h

2: 70.5 percent / dithionite,aq. sodium chloride / CHCl₃ / 0.03 h / acetate buffer

3: 37.8 percent / 24 h

With sodium hydrogencarbonate; dithionite^(2-); 3-chloro-benzenecarboperoxoic acid; sodium chloride; In chloroform;
DOI:10.1021/ja00352a045