4-(3-(4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)phenyl)prop-2-enoyl)benzonitrile

Base Information

Chemical Name:4-(3-(4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)phenyl)prop-2-enoyl)benzonitrile
CAS No.:1335107-26-0
Molecular Formula:C₃₆H₄₆N₂O₅S₃
Molecular Weight:682.97
Hs Code.:

Synonyms:4-(3-(4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)phenyl)prop-2-enoyl)benzonitrile

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Chemical Property of 4-(3-(4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)phenyl)prop-2-enoyl)benzonitrile

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Technology Process of 4-(3-(4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)phenyl)prop-2-enoyl)benzonitrile

There total 8 articles about 4-(3-(4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)phenyl)prop-2-enoyl)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1443-80-7
4-cyanophenyl methyl ketone

: 1335107-25-9
4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)benzaldehyde

: 1335107-26-0
4-(3-(4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)phenyl)prop-2-enoyl)benzonitrile

Guidance literature:: With pyrrolidine; In ethanol; benzene; at 50 ℃; for 48h;
DOI:10.1021/ja207004v

Reference yield:

: 1335107-23-7
bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane

: 1335107-26-0
4-(3-(4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)phenyl)prop-2-enoyl)benzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 24 h / 85 °C

2: pyrrolidine / ethanol; benzene / 48 h / 50 °C

With pyrrolidine; caesium carbonate; In ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ja207004v

Reference yield:

: 120-07-0
2,2'-(phenylimino)bis[ethanol]

: 1335107-26-0
4-(3-(4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)phenyl)prop-2-enoyl)benzonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / N,N-dimethyl-formamide / 4 h / 90 °C / Cooling

2: sodium iodide / butanone / 24 h / 65 °C

3: caesium carbonate / water; N,N-dimethyl-formamide / 24 h / 85 °C

4: pyrrolidine / ethanol; benzene / 48 h / 50 °C

With pyrrolidine; caesium carbonate; sodium iodide; trichlorophosphate; In ethanol; water; N,N-dimethyl-formamide; butanone; benzene;
DOI:10.1021/ja207004v