bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane

Base Information

Chemical Name:bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane
CAS No.:1335107-23-7
Molecular Formula:C₃₀H₄₂O₄S₃
Molecular Weight:562.859
Hs Code.:

Synonyms:bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane

Suppliers and Price of bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane

There total 3 articles about bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1335107-22-6
5-((benzylthio)methyl)-5-bromomethyl-2,2-dimethyl-1,3-dioxane

: 1335107-23-7
bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane

Guidance literature:: With sodiumsulfide nonahydrate; sodium hydrogencarbonate; potassium iodide; In water; N,N-dimethyl-formamide; at 90 ℃; for 20h; Inert atmosphere;
DOI:10.1021/ja207004v

Reference yield:

: 43153-20-4
5,5-bis-bromomethyl-2,2-dimethyl-[1,3]dioxane

: 1335107-23-7
bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane

Guidance literature:: Multi-step reaction with 3 steps

1: sodiumsulfide nonahydrate; sodium hydrogencarbonate; potassium iodide / methanol; water / 36 h / Reflux

2: potassium carbonate / acetonitrile / 48 h / 60 °C / Inert atmosphere

3: sodiumsulfide nonahydrate; sodium hydrogencarbonate; potassium iodide / water; N,N-dimethyl-formamide / 20 h / 90 °C / Inert atmosphere

With sodiumsulfide nonahydrate; sodium hydrogencarbonate; potassium carbonate; potassium iodide; In methanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja207004v

Reference yield:

: 156720-48-8
7,7-dimethyl-6,8-dioxa-2-thiaspiro[3.5]nonane

: 1335107-23-7
bis((5-((benzylthio)methyl)-2,2-dimethyl-1,3-dioxan-5-yl)methyl)sulfane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 48 h / 60 °C / Inert atmosphere

2: sodiumsulfide nonahydrate; sodium hydrogencarbonate; potassium iodide / water; N,N-dimethyl-formamide / 20 h / 90 °C / Inert atmosphere

With sodiumsulfide nonahydrate; sodium hydrogencarbonate; potassium carbonate; potassium iodide; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja207004v