methyl (2S)-2-((2-(bis-(tert-butoxycarbonylmethyl)amino)-ethyl)-(tert-butoxycarbonylmethyl)-amino)-3-(4-tertbutoxy-phenyl)-propionate

Base Information

Chemical Name:methyl (2S)-2-((2-(bis-(tert-butoxycarbonylmethyl)amino)-ethyl)-(tert-butoxycarbonylmethyl)-amino)-3-(4-tertbutoxy-phenyl)-propionate
CAS No.:1278457-65-0
Molecular Formula:C₃₄H₅₆N₂O₉
Molecular Weight:636.827
Hs Code.:

Synonyms:methyl (2S)-2-((2-(bis-(tert-butoxycarbonylmethyl)amino)-ethyl)-(tert-butoxycarbonylmethyl)-amino)-3-(4-tertbutoxy-phenyl)-propionate

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Chemical Property of methyl (2S)-2-((2-(bis-(tert-butoxycarbonylmethyl)amino)-ethyl)-(tert-butoxycarbonylmethyl)-amino)-3-(4-tertbutoxy-phenyl)-propionate

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Technology Process of methyl (2S)-2-((2-(bis-(tert-butoxycarbonylmethyl)amino)-ethyl)-(tert-butoxycarbonylmethyl)-amino)-3-(4-tertbutoxy-phenyl)-propionate

There total 1 articles about methyl (2S)-2-((2-(bis-(tert-butoxycarbonylmethyl)amino)-ethyl)-(tert-butoxycarbonylmethyl)-amino)-3-(4-tertbutoxy-phenyl)-propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1278457-61-6
methyl (2S)-2-(tert-butoxycarbonylmethyl-amino)-3-(4-tert-butoxy-phenyl)-propionate

: 146432-43-1
N-(2-bromoethyl)-N-[2-(1,1-dimethylethoxy)-2-oxoethyl]glycine 1,1-dimethylethyl ester

: 1278457-65-0
methyl (2S)-2-((2-(bis-(tert-butoxycarbonylmethyl)amino)-ethyl)-(tert-butoxycarbonylmethyl)-amino)-3-(4-tertbutoxy-phenyl)-propionate

Guidance literature:: With sodium carbonate; In acetonitrile; for 48h; Reflux;
DOI:10.1016/j.bmc.2010.07.064

Reference yield:

: 1278457-65-0
methyl (2S)-2-((2-(bis-(tert-butoxycarbonylmethyl)amino)-ethyl)-(tert-butoxycarbonylmethyl)-amino)-3-(4-tertbutoxy-phenyl)-propionate

: (2S)-2-((2-(bis-carboxymethyl-amino)-ethyl)-carboxymethyl-amino)-3-(4-hydroxy-phenyl)-propionic acid

Guidance literature:: methyl (2S)-2-((2-(bis-(tert-butoxycarbonylmethyl)amino)-ethyl)-(tert-butoxycarbonylmethyl)-amino)-3-(4-tertbutoxy-phenyl)-propionate; With water; potassium hydroxide; In methanol; at 20 ℃; for 8h;

In methanol; water; pH=2; Acidic conditions;

With chlorotriisopropylsilane; trifluoroacetic acid; In chloroform; at 20 ℃; for 18h;
DOI:10.1016/j.bmc.2010.07.064