Thiophosphorous acid O-{(2R,3S,5R)-5-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester S-ethyl ester O'-methyl ester

Base Information

Chemical Name:Thiophosphorous acid O-{(2R,3S,5R)-5-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester S-ethyl ester O'-methyl ester
CAS No.:102538-03-4
Molecular Formula:C₄₁H₄₃N₂O₉PS
Molecular Weight:770.84
Hs Code.:

Thiophosphorous acid O-{(2R,3S,5R)-5-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester S-ethyl ester O'-methyl ester

Synonyms:Thiophosphorous acid O-{(2R,3S,5R)-5-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester S-ethyl ester O'-methyl ester

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Chemical Property of Thiophosphorous acid O-{(2R,3S,5R)-5-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester S-ethyl ester O'-methyl ester

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Technology Process of Thiophosphorous acid O-{(2R,3S,5R)-5-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester S-ethyl ester O'-methyl ester

There total 1 articles about Thiophosphorous acid O-{(2R,3S,5R)-5-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester S-ethyl ester O'-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 102573-69-3
5'-O-(4-4'-dimethoxytrityl)-N³-benzoyl thymidine

: C₃H₈ClOPS

: 102538-03-4
Thiophosphorous acid O-{(2R,3S,5R)-5-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester S-ethyl ester O'-methyl ester

Guidance literature:: In pyridine; for 0.166667h; Ambient temperature;
DOI:10.1021/ja00273a049

Reference yield:

: 94189-81-8
3,3'-O,N-dibenzoylthymidine

: 102538-03-4
Thiophosphorous acid O-{(2R,3S,5R)-5-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester S-ethyl ester O'-methyl ester

: 130983-93-6
C₆₃H₅₉N₄O₁₆P

Guidance literature:: With lutidine; silver(I) acetate; triethylamine; In dichloromethane; for 0.0333333h;
DOI:10.1021/ja00273a049

Reference yield:

: 94189-81-8
3,3'-O,N-dibenzoylthymidine

: 102538-03-4
Thiophosphorous acid O-{(2R,3S,5R)-5-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl} ester S-ethyl ester O'-methyl ester

: 102538-11-4
methyl 5'-O-dimethoxytrityl-N³-benzoylthymidin-3'-yl N³,3'-O-dibenzoylthymidin-5'-yl phosphate

Guidance literature:: With 2,6-dimethylpyridine; lutidine; water; iodine; silver(I) acetate; triethylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, 2 min, 2.) CH₂Cl₂, THF;
DOI:10.1021/ja00273a049