ethylthio 6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

Base Information

Chemical Name:ethylthio 6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside
CAS No.:1259036-11-7
Molecular Formula:C₃₆H₄₅N₃O₇SSi
Molecular Weight:691.921
Hs Code.:

Synonyms:ethylthio 6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

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Chemical Property of ethylthio 6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

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Technology Process of ethylthio 6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

There total 1 articles about ethylthio 6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 289712-58-9
2-(azidomethyl)benzoyl chloride

: 460741-89-3
ethylthio 2-O-benzoyl-4-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranoside

: 1259036-11-7
ethylthio 6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1039/c0cc03153d

Reference yield:

: 1259036-11-7
ethylthio 6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

: 6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranose

: 1259036-12-8
6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranose

Guidance literature:: ethylthio 6-O-(2-(azidomethyl)benzoyl)-2-O-benzoyl-4-O-benzyl-3-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside; With N-iodo-succinimide; In water; acetone; at 0 ℃; for 0.166667h;

With triethylamine; In water; acetone; at 20 ℃; for 1h; optical yield given as %de;
DOI:10.1039/c0cc03153d