2-(trimethylsilanyl)ethanesulfonic acid (2-nitrophenyl)amide

Base Information

• Chemical Name: 2-(trimethylsilanyl)ethanesulfonic acid (2-nitrophenyl)amide
• CAS No.: 1045771-53-6
• Molecular Formula: C₁₁H₁₈N₂O₄SSi
• Molecular Weight: 302.426
• Mol file: 1045771-53-6.mol

Synonyms:2-(trimethylsilanyl)ethanesulfonic acid (2-nitrophenyl)amide

Chemical Property of 2-(trimethylsilanyl)ethanesulfonic acid (2-nitrophenyl)amide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2-(trimethylsilanyl)ethanesulfonic acid (2-nitrophenyl)amide

There total 1 articles about 2-(trimethylsilanyl)ethanesulfonic acid (2-nitrophenyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-nitrophenyl bromide (577-19-5) + 2-(trimethylsilyl)ethanesulfonamide (125486-96-6) → 2-(trimethylsilanyl)ethanesulfonic acid (2-nitrophenyl)amide (1045771-53-6)

Guidance literature:

With caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 100 ℃; for 15h;

DOI:10.1016/j.tetlet.2008.05.099

Reference yield: 87.0%

2-(trimethylsilanyl)ethanesulfonic acid (2-nitrophenyl)amide (1045771-53-6) → 2-nitro-aniline (88-74-4)

Guidance literature:

With cesium fluoride; In N,N-dimethyl-formamide; at 130 ℃; for 36h;

DOI:10.1016/j.tetlet.2008.05.099

upstream raw materials:

2-nitrophenyl bromide

2-(trimethylsilyl)ethanesulfonamide

Downstream raw materials:

2-nitro-aniline

Refernces