tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate

Base Information

Chemical Name:tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate
CAS No.:873005-95-9
Molecular Formula:C₂₆H₃₆F₃NO₄Si
Molecular Weight:511.657
Hs Code.:

Synonyms:tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate

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Chemical Property of tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate

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Technology Process of tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate

There total 1 articles about tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 873005-93-7
tert-butyl 2-hydroxy-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 873005-95-9
tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield: 94.0%

: 873005-95-9
tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate

: 873004-41-2
tert-Butyl 2-hydroxy-6-({4-[methyl(methylsulfonyl)amino]phenoxy}methyl)-3-(trifluoromethyl)benzoate

Guidance literature:: tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate; With methanesulfonyl chloride; triethylamine; In dichloromethane; at 20 ℃;

With methanol; tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 6h;

Reference yield: 66.0%

: 873005-95-9
tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate

: 5239-82-7
cyclopropylacetic acid

: 873004-33-2
tert-butyl 6-({4-[(cyclopropylacetyl)(methyl)amino]phenoxy}methyl)-2-hydroxy-3-(trifluoromethyl)benzoate

Guidance literature:: tert-butyl 2-{[tert-butyl(dimethyl)silyl]oxy}-6-{[4-(methylamino)phenoxy]methyl}-3-(trifluoromethyl)benzoate; cyclopropylacetic acid; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; dichloromethane; at 20 ℃; for 6h;