tertiary butyl 3-((3,4-dichlorophenyl)(phenoxy)methyl)azetidine-1-carboxylate

Base Information

Chemical Name:tertiary butyl 3-((3,4-dichlorophenyl)(phenoxy)methyl)azetidine-1-carboxylate
CAS No.:1398705-28-6
Molecular Formula:C₂₁H₂₃Cl₂NO₃
Molecular Weight:408.325
Hs Code.:

Synonyms:tertiary butyl 3-((3,4-dichlorophenyl)(phenoxy)methyl)azetidine-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tertiary butyl 3-((3,4-dichlorophenyl)(phenoxy)methyl)azetidine-1-carboxylate

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Technology Process of tertiary butyl 3-((3,4-dichlorophenyl)(phenoxy)methyl)azetidine-1-carboxylate

There total 4 articles about tertiary butyl 3-((3,4-dichlorophenyl)(phenoxy)methyl)azetidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1398705-03-7
tertiary butyl 3-((3,4-dichlorophenyl)(hydroxy)methyl)azetidine-1-carboxylate

: 108-95-2,27073-41-2
phenol

: 1398705-28-6
tertiary butyl 3-((3,4-dichlorophenyl)(phenoxy)methyl)azetidine-1-carboxylate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 24h;

Reference yield:

: 177947-96-5
tert-butyl 3-formylazetidine-1-carboxylate

: 1398705-28-6
tertiary butyl 3-((3,4-dichlorophenyl)(phenoxy)methyl)azetidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 3 h / 0 °C

1.2: 1 h / 0 - 20 °C

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 24 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran;

Reference yield:

: 142253-55-2
1-(t-butyloxycarbonyl)-azetidine-3-carboxylic acid

: 1398705-28-6
tertiary butyl 3-((3,4-dichlorophenyl)(phenoxy)methyl)azetidine-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 0 °C

1.2: 0.5 h / 0 - 20 °C

2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 3 h / -78 °C

2.2: 1 h / -78 °C

3.1: tetrahydrofuran / 3 h / 0 °C

3.2: 1 h / 0 - 20 °C

4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 24 h / 0 - 20 °C

With oxalyl dichloride; di-isopropyl azodicarboxylate; dimethylsulfide borane complex; dimethyl sulfoxide; triphenylphosphine; In tetrahydrofuran; dichloromethane;