10-(5-Chloro-4-cyclohex-1-en-1-yl-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine

Base Information

• Chemical Name: 10-(5-Chloro-4-cyclohex-1-en-1-yl-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine
• CAS No.: 473574-30-0
• Molecular Formula: C₂₆H₂₅ClN₂O₂
• Molecular Weight: 432.95

Synonyms:10-(5-Chloro-4-cyclohex-1-en-1-yl-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine

Chemical Property of 10-(5-Chloro-4-cyclohex-1-en-1-yl-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine

Chemical Property:

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Technology Process of 10-(5-Chloro-4-cyclohex-1-en-1-yl-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine

There total 2 articles about 10-(5-Chloro-4-cyclohex-1-en-1-yl-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(10,11-Dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepin-10-yl)-[5-chloro-2-methoxy-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-methanone (473574-29-7) + cyclohex-1-en-1-yl trifluoromethane sulfonate (28075-50-5) + sodium carbonate (497-19-8) → 10-(5-Chloro-4-cyclohex-1-en-1-yl-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine (473574-30-0)

Guidance literature:

In diethyl ether; hexane; ethyl acetate; N,N-dimethyl-formamide; Petroleum ether;

Reference yield:

(10,11-Dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepin-10-yl)-[5-chloro-2-methoxy-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-methanone (473574-29-7) + (10,11-Dihydro-5H-pyrrolo[2,1-c[1,4]benzodiazepin-10-yl)-[5-chloro-2-methoxy-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-methanone + cyclohex-1-en-1-yl trifluoromethane sulfonate (28075-50-5) + sodium carbonate (497-19-8) → 10-(5-Chloro-4-cyclohex-1-en-1-yl-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine (473574-30-0)

Guidance literature:

In diethyl ether; hexane; ethyl acetate; N,N-dimethyl-formamide; Petroleum ether;

Reference yield:

3-oxo-2-methyl-cylclohex-1-en-1-yl trifluoromethanesulfonate + (10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-methanone (473596-71-3) + 10-(5-Chloro-4-cyclohex-1-en-1-yl-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine (473574-30-0) → 3-[4-(10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-phenyl]-2-methyl-cyclohex-2-en-1-one + Petroleum ether

Guidance literature:

In hexane; ethyl acetate;

upstream raw materials:

(10,11-Dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepin-10-yl)-[5-chloro-2-methoxy-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-methanone

cyclohex-1-en-1-yl trifluoromethane sulfonate

sodium carbonate

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